2025 年 1 月
特别关注:水力压裂

使用超高分辨率纳米粒子示踪剂进行集群级流动映射和生产诊断

现有的穿孔或集群级生产监测方法通常具有挑战性、侵入性强且成本高昂。本案例研究概述了一种新型流量监测技术和改进的穿孔系统,该系统保持了与不使用示踪剂的传统系统类似的性能,同时还消除了额外的处理和监管负担。 

华莱士·亨德里克斯 (WALLACE HENDRICKS),True Oil LLC;埃里克·马歇尔 (ERIC MARSHALL),GEODynamics;塔尔加特·绍卡诺夫 (TALGAT SHOKANOV),约翰·奥利弗 (JOHN OLIVER) 和郭全 (QUAN GUO),QuantumPro, Inc. 

过去二十年来,非常规完井效率的技术进步一直在稳步推进。一些较为著名的进步包括: 

  • 增加级数,以更精确地定位裂缝并改善储层接触 
  • 塞式射孔完井,实现分级隔离和顺序压裂 
  • 引入相等的入孔射孔弹,可实现更高的流体和支撑剂分布均匀性 
  • 高速滑溜水压裂,实现更经济高效的支撑剂输送 
  • 工程支撑剂更加坚固,可提高裂缝性能和长期产量 
  • 先进的建模和模拟,可以更好地了解裂缝扩展和流体流动行为的建模 
  • 光纤传感、井下摄像机和改进的压力诊断技术。 

所有这些进步都推动了超低渗透非常规油气藏油气生产的革命,极大地改变了整个行业。虽然这一进步备受瞩目,但利润压力不断缩小,要求运营商继续实现更好的经济效益、提高采收率并缩短从一口井到下一口井的周转时间。因此,技术进步仍在继续,挑战运营商进行创新、争夺投资、展示渐进式改进并挑战现状。 

对于寻求提高财务回报的上游运营商而言,提高完井效率是一项艰巨的挑战。完井效率的逐步提高越来越依赖于对可变源岩的了解。这种了解使得完井计划能够考虑到岩性变化——甚至是阶段层面的变化。通过更精确地调整射孔策略,运营商可以改善支撑剂分布并提高整体井性能。 

人们曾经认为,井段和穿孔簇最好沿着目标地层水平面均匀分布。然而,它们的产量往往变化很大,这凸显了更彻底的地下检查的必要性。井距和加密计划也需要对地下有更深入的了解,以最大限度地扩大面积并避免昂贵的井间通信。穿孔位置、密度、大小和方向等因素以及压裂阶段和间距以及压裂液和支撑剂的选择都会对结果产生重大影响。获取必要的数据可能很复杂、昂贵且通常遥不可及,投资回报也不确定。 

先进的测井和成像工具扩大了我们对地下的了解。然而,它们的高部署成本以及工具故障和数据丢失的风险可能带来经济挑战。所获取信息的价值往往没有得到充分理解,导致问题多于答案。由于后勤约束和井下限制,部署这些工具也涉及复杂性。这需要在井场增加工作人员,延长钻机时间,从而增加成本。较新的测井工具提供了更好的稳健性、效率和成本效益,但它们的高初始成本和有限的长期数据可能仍然具有挑战性——尤其是对于利润微薄的运营商而言。 

微地震监测用于绘制诱发裂缝,可提供可操作的见解。然而,流动剖面分辨率有限,成本效益分析可能具有挑战性。虽然成本降低使微地震监测更加容易实现,但它仍然有局限性。在压裂过程中注入的化学和放射性示踪剂很有用,但也有缺点,包括成本高、储层岩石吸收率高以及需要特殊处理。 

操作员越来越需要对地下有更深入的了解,以便更智能地对地层进行射孔和压裂,并回答许多关键问题。例如:如果井径偏离设计路径 10 英尺或更多,对某个区域进行射孔和压裂是否仍然有效?射孔孔径、穿透力和簇间距是否最佳,后续井在什么时候需要进行调整?井间通信是否存在?如果有,如何确认井间通信?通过额外数据采集实现的更深入理解可以对这些问题提供更多见解,并指导决策、测试假设并带来持续改进和更高的投资回报率 (ROI)。 

评估射孔流动性能的价值 

评估长水平井中的穿孔流动性能对于优化油气完井至关重要。在长水平井中,必须确保水力压裂液和支撑剂均匀分布在所有穿孔簇中。分析流动有助于识别可能导致裂缝生长不均匀和刺激水平不理想的任何限制或优先路径。 

通过穿孔实现高效流动可改善井筒与储层之间的连通,从而最大程度地扩大压裂液和支撑剂的接触面积,提高碳氢化合物的采收率。通过分析穿孔流动性能,操作员可以精确定位流动受限的区域。这些信息对于调整未来油井完井参数的决策非常有价值,包括: 

  • 穿孔密度:增加低流量区域的穿孔数量或完全跳过区域。 
  • 射孔系统:修改枪直径、定位射孔和改变装药类型,以最大限度地提高流体和支撑剂分布的均匀性。 
  • 阶段间距:调整阶段之间的距离以优化流体分布并最大限度提高产量。 

了解射孔流动性能有助于运营商避免在自然流量大的地区过度投入增产,从而更有效地分配资源。射孔高效流动还可最大限度地减少井筒压力下降,从而提高生产率并降低提升成本。 

此外,优化的射孔流动性能有助于防止支撑剂筛出,从而防止支撑剂筛出,从而损坏地层、阻碍生产并导致昂贵的干预。分析流动还可以帮助识别套管或水泥中的潜在泄漏点或薄弱区域,确保井的完整性并防止环境问题。 

通过射孔系统传送超高分辨率纳米粒子示踪剂,一个新前沿 

纳米粒子示踪剂代表了生产和流量监测能力的重大进步。它们比化学或放射性示踪剂更坚固,能够承受极端井况,无需特殊处理。在穿孔或簇级,这些示踪剂提供更详细的测量,增加了新的维度和大量以前现有测量无法实现的应用。纳米粒子示踪剂提供了有关地质信息和变异性的重要见解。随着石油和天然气行业寻求提高效率和最大限度地提高采收率,这些纳米粒子通过提供有关储层行为的宝贵见解,具有发挥越来越重要作用的巨大机会。 

考虑到传统方法的成本、复杂性和局限性,QuantumPro, Inc. 设想使用通过射孔弹输送的纳米粒子示踪剂,作为行业已准备好迎接的机遇和创新。本文讨论的具体应用——评估射孔流动性能——是正在评估、成功测试和部署的新方法之一。纳米粒子示踪剂技术为评估完井效率提供了新的细节水平,超过了传统测量的规模和细节。 

独特可识别的惰性纳米粒子示踪剂可实现广泛应用 

QuantumPro 的 FloTrac 超高分辨率纳米粒子示踪剂可配置多达 220 种不同的、可唯一识别的惰性变体,图 1。这种独特的示踪剂的庞大组合可实现广泛的应用,可以扩展到相邻井,记录井间通信(对于优化井距至关重要),并用数据驱动的优化取代反复试验的方法。

图 1. FloTrac 示踪剂与不同沙粒的尺寸比较。

 

与液体化学示踪剂不同,每种 FloTrac 纳米颗粒示踪剂都与水和油兼容,只需一种示踪剂成分,而不受流体流的影响,从而大大降低了成本。由于不溶性 FloTrac 示踪剂在部署后不会溶解,操作员可以进行表面采样至少九个月——远远超出了液体化学示踪剂的能力。FloTrac 示踪剂在高达 2,000 °F 的温度下也能保持稳定性。 

这种专门设计的纳米粒子具有广泛的应用前景,经过实验室测试后,True Oil, LLC最近在北达科他州威利斯顿盆地通过改进的射孔弹进行了首次现场试验,并取得了令人鼓舞的结果。 

纳米粒子示踪剂在射孔系统中的应用实验室验证 

2023 年,研究人员根据 API RP19 标准,在位于德克萨斯州米尔萨普的 GEODynamics Inc. 测试和制造工厂通过全面的实验室测试验证了纳米颗粒示踪剂和实施方法。研究人员将纳米颗粒示踪剂添加到等入射孔 FracIQ 炸药的穿孔衬管中,如图 2 所示。 

图 2. 添加到穿孔衬管的超高分辨率纳米粒子。

该测试旨在实现以下目标: 

  • 评估纳米粒子示踪剂在射孔弹爆炸典型极端条件下的稳定性 
  • 确定使用纳米颗粒是否对穿孔尺寸和穿透深度产生影响,以及不同纳米颗粒浓度如何影响炸药爆炸后的相应测量结果 
  • 确认纳米颗粒的回收率、可检测性和测量浓度 

试验证实,纳米粒子示踪剂能够承受射孔爆炸的极端条件。重要的是,应用于射孔衬套的纳米粒子的试验浓度对预期穿透深度和入口孔尺寸的影响微乎其微——这是维持装药性能的关键因素。 

对从混凝土芯内部的穿孔隧道收集的流体和固体颗粒样品进行高能亚原子 X 射线分析,结果表明各种电荷类型的示踪剂回收率高且信号特性良好。不同的示踪剂浓度允许选择用于现场部署的最佳浓度。纳米颗粒检测得到确认,并可进行现场测试。 

通过实验室测试验证了该方法后,研究人员进行了现场试验,以确认纳米粒子示踪剂和输送机制的实际应用。 

现场测试验证应用和方法 

与实验室测试一样,现场试验的目的是探索各种纳米颗粒浓度并验证可测量的纳米颗粒回收率,包括现场试验中的表面回收率。现场试验还允许将纳米颗粒不仅应用于穿孔衬管,还应用于概述的穿孔系统的其他区域。第一阶段现场测试于 2024 年 10 月在威利斯顿盆地的 True Oil, LLC 运营的油井中进行。 

QuantumPro, Inc. 团队将五种独特的纳米粒子示踪剂送到 GEODynamics 制造工厂进行准备并运送到井场。制造商事先做好了准备,因此一旦射孔枪到达现场,除了将枪放置在预定位置外,无需进行特殊工作,因为纳米粒子示踪剂具有唯一可识别性,操作员可以将采收与特定射孔或射孔簇联系起来。该团队设计了一项现场测试,将完井阶段 12 和 13 确定为代表性阶段,每个阶段测试八个射孔簇。 

图 3. 现场测试标准概述,确定了如何部署五种独特的示踪剂以及测试的不同浓度。

现场测试包括实验室测试之外的额外可变性,以研究更广泛的应用,包括在枪内可用空间的小瓶中放置相对大量的纳米粒子示踪剂。与实验室测试一样,应用不同的纳米粒子示踪剂浓度来确定示踪剂回收率。每个阶段由八个簇组成,每个簇用四发子弹射孔。使用标准的插入和射孔方法部署了嵌入示踪剂的炸药,制造合作伙伴 GEODynamics 在制造过程中集成了纳米粒子示踪剂,图 3。 

 

研究结果鼓励后续检测 

结果表明,在簇级别上纳米粒子示踪剂的回收率足够,有利于对每个簇进行高级流动映射、产量量化和流动性能验证,图 4。 

图4. 首次生产后一周采集的返排样品的结果和分析。

现场试验成功后,该团队启动了第二阶段现场测试,该测试正在第二口 True Oil 井中进行,结果将于 2025 年 1 月下旬公布。作为对流程和结果的进一步验证,True Oil 代表 Wallace Hendricks 评论说,“能够轻松部署并控制单个示踪剂在特定区域的位置,这是一个改变游戏规则的能力。”他补充道,“在现场,示踪剂的部署与有线操作无缝衔接。无需额外的人员或设备。” 

 

生产流程监控领域的突破性、成本效益的进步 

簇级流量监测技术标志着行业取得突破性进展,为评估穿孔流量性能和井间通信提供了经济高效且非侵入式的手段。此外,该技术还允许操作员: 

  • 实现簇级流动映射分辨率,为除降压测试之外的穿孔效率提供进一步验证 
  • 验证单井中多种穿孔设计的穿孔效率,以补充其他诊断方法(如摄像机或光纤)的结果或减少对其他诊断方法的依赖 
  • 更好地了解区域外地质层的阶段性贡献 
  • 验证区域隔离和封堵及水泥质量
  • 了解脚趾与中跟的贡献。 

在射孔隧道中嵌入纳米颗粒示踪剂的早期部署意味着操作员不仅可以更好地了解哪些簇有贡献,还可以更好地了解压裂如何分布以及如何对井的整体产量做出贡献。 

该方法的应用范围扩展到非常规井、海上井、增强型地热系统 (EGS) 井和碳捕获、利用和储存 (CCUS) 井的多阶段完井。穿孔水平流量监测方法提高了穿孔后分析和油藏开发过程中的清晰度,为优化穿孔设计和整体完井策略提供了关键见解,从而最大限度地提高资产价值和绩效。 

致谢 

作者真诚感谢 GEODynamics 前员工 Phil Snider 和 Steve Baumgartner,他们的支持和贡献对这项技术起到了至关重要的作用。 

华莱士·亨德里克斯 (WALLACE HENDRICKS)是 True Oil LLC 的完井主管。他拥有怀俄明大学地球物理学和土木工程学士学位。他还是怀俄明州注册的专业工程师。 

 

 

 

埃里克·马歇尔 (ERIC MARSHALL)是一名石油工程师,在石油和天然气行业拥有 23 年的经验,专门从事水力压裂和油藏工程。他目前担任 GEODynamics 的高级技术顾问,负责寻找新技术和知识产权以推动未来增长。在加入 GEODynamics 之前,马歇尔先生曾担任 FractureID 的工程副总裁,并在那里建立了一个工程咨询部门。他还管理了哈里伯顿在 11 个国家/地区的连续油管增产服务的全球技术实施团队。马歇尔先生拥有科罗拉多矿业学院机械工程学士学位,是多个州的注册专业石油工程师。他积极参与 SPE 等专业组织。 

 

TALGAT SHOKANOV是 QuantumPro, Inc. 的首席执行官,他在 SLB 工作了 15 年后于 2017 年创立了该公司。在 SLB,他担任过各种国际和技术开发职务,之前曾领导过 SLB 通过水力压裂业务线进行岩屑回注,包括地下工程、处置域测绘和压力诊断分析。他拥有多项专利,并撰写了 50 多篇复杂压裂和注入方面的技术论文。他拥有哈萨克斯坦萨特巴耶夫大学石油工程学士和硕士学位。 

 

约翰·奥利弗 (JOHN OLIVER) 是 QuantumPro Inc. 的业务顾问。他在石油和天然气行业拥有超过 45 年的经验,包括在 SLB 公司 MI SWACO 担任多个高级管理职位。他曾担任高级副总裁,管理南美业务部门的所有部门,并担任全球营销经理。奥利弗先生后来领导 Prince International 的一个部门 Prince Energy,并于 2018 年 7 月从该部门退休。他目前在多家董事会任职,并担任多家公司和能源私募股权投资公司的顾问。他拥有苏格兰圣安德鲁斯大学生物化学荣誉学士学位。

 

QUAN GUO是 QuantumPro, Inc. 的地质力学顾问。他曾在 2003 年至 2022 年期间就职于 MI SWACO,后来又在 SLB 任职。在加入 MI SWACO 之前,他曾在 2000 年至 2003 年就职于 Advantek,在 1992 年至 2000 年就职于 TerraTek。他的经验包括射孔和水力压裂实验室测试和建模、钻井液和井筒加固、岩屑和采出水回注。他拥有 13 项专利,并撰写了 80 多篇技术论文。他拥有兰州大学数学和力学学士学位、中国华中科技大学工程力学硕士学位以及伊利诺伊州埃文斯顿西北大学机械工程博士学位。 

相关文章 档案中的资料
原文链接/WorldOil
January 2025
SPECIAL FOCUS: HYDRAULIC FRACTURING

Cluster-level flow mapping and production diagnostics using ultrahigh-resolution nanoparticle tracers

Existing methods for perforation or cluster-level production monitoring are often challenging, intrusive and costly. This case study outlines a novel flow monitoring technique and modified perforating system, which maintains similar performance to conventional systems without tracers, while also eliminating additional handling and regulatory burdens. 

WALLACE HENDRICKS, True Oil LLC; ERIC MARSHALL, GEODynamics; TALGAT SHOKANOV, JOHN OLIVER and QUAN GUO, QuantumPro, Inc. 

Technological advancements in unconventional well completion efficiency have been on a steady march over the last two decades. Some of the more well-known advancements have included: 

  • Increased stages for more precise placement of fractures and better reservoir contact 
  • Plug-and-perf completions, enabling stage isolation and sequential fracturing 
  • Introduction of equal entry hole perforating charges that yield higher uniformity of fluid and proppant distribution 
  • High-rate slickwater fracs, yielding more economically efficient proppant transport 
  • Engineered proppants that are more robust, to enhance fracture performance and long-term production 
  • Advanced modeling and simulation, allowing better insight into fracture propagation and modeling of fluid flow behavior 
  • Fiber optic sensing, downhole cameras, and improved pressure diagnostic techniques. 

All these advancements contributed to a revolution in oil and gas production in ultra-low permeability unconventional reservoirs, dramatically transforming the industry. While this progress has been heralded, ever-tight margin pressure demands that operators continue to achieve better economic efficiency, increase recovery and improve turnaround time from one well to the next. As a result, the technological march continues, challenging operators to innovate, compete for investment, demonstrate incremental improvements, and challenge the status quo. 

Enhancing well completions efficiency is a difficult challenge for upstream operators seeking to improve financial returns. Incremental improvements in completions efficiency increasingly depend on understanding the variable source rock. This understanding allows for completion programs that account for lithology variations—even at the stage level. By tailoring the perforation strategy more precisely, operators can improve proppant distribution and enhance overall well performance. 

Well stages and perforation clusters were once thought to be best distributed evenly along the target formation lateral. However, they often produce at highly variable rates, highlighting the need for more thorough subsurface inspection. Well spacing and infill programs also require greater subsurface understanding, to maximize acreage and avoid costly cross-well communication. Factors like perforation placement, density, size and orientation—along with frac stages and spacing and frac fluid and proppant selection—can significantly impact results. Acquiring the necessary data can be complex, expensive and often out of reach, with an uncertain return on investment. 

Advanced logging and imaging tools have expanded our understanding of the subsurface. However, their high deployment cost and the risk of tool failure and data loss can pose economic challenges. The value of the acquired information is often not fully understood, leading to more questions than answers. Deploying these tools also involves complexities, due to logistical constraints and downhole limitations. This necessitates additional staff at the wellsite, increasing costs by extending rig time. Newer logging tools offer improved robustness, efficiency and cost-effectiveness, but their high initial cost and limited long-term data may still be challenging—particularly for operators working with tight margins. 

Microseismic monitoring, used to map induced fractures, delivers actionable insight. However, flow profile resolution is limited, and the cost-benefit analysis can be challenging. While cost reductions are making microseismic monitoring more accessible, it still has limitations. Chemical and radioactive tracers—injected during fracturing—are useful but also have drawbacks, including high costs, high absorption to the reservoir rock and a need for special handling. 

Operators increasingly require a deeper understanding of the subsurface to more intelligently perf and frac a formation and answer many key questions. For example: is it still effective to perf and frac a zone, if the well path strays 10 ft or more from the designed path? Are the perforation hole size, penetration, and cluster spacing optimal, and at what point are adjustments needed in successive wells? Is there cross-well communication? If so, how can cross-well communication be confirmed? A deeper understanding, enabled by additional data acquisition, can deliver more insight into questions like these, as well as guide decisions, test hypotheses and lead to continued improvements and higher return on investment (ROI). 

THE VALUE OF ASSESSING PERFORATION FLOW PERFORMANCE 

Assessing perforation flow performance in long laterals is crucial for optimizing oil and gas completions. In long laterals, it's essential to ensure that hydraulic fracturing fluid and proppants are distributed evenly across all perforation clusters. Analyzing flow helps to identify any restrictions or preferential paths that could lead to uneven fracture growth and suboptimal levels of stimulation. 

Efficient flow through perforations improves communication between the wellbore and the reservoir, maximizing the area contacted by the fracturing fluid and proppant and leading to improved hydrocarbon recovery. By analyzing perforation flow performance, operators can pinpoint zones where flow is restricted. This information is valuable in making the decision to adjust completion parameters in future wells, including: 

  • Perforation density: increasing the number of perforations in low-flow zones or skipping zones altogether. 
  • Perforating systems: modifying gun diameters, orienting perforations and changing charge types to maximize the uniformity of fluid and proppant distribution. 
  • Stage spacing: adjusting the distance between stages to optimize fluid distribution and maximize production. 

Understanding perforation flow performance helps operators avoid overspending on stimulation in zones with naturally high flow capacity, allowing for more efficient allocation of resources. Efficient flow through perforations also minimizes pressure drop along the wellbore, leading to improved production rates and lower lifting costs. 

Furthermore, optimized perforation flow performance helps prevent proppant screen-outs, which can damage the formation, hinder production and lead to costly intervention. Analyzing flow also can help identify potential leak points or areas of weakness in the casing or cement, ensuring well integrity and preventing environmental issues. 

ULTRAHIGH-RESOLUTION NANOPARTICLE TRACERS DELIVERED VIA PERFORATION SYSTEMS, A NEW FRONTIER 

Nanoparticle tracers represent a significant advancement in production and flow monitoring capability. They are more robust than chemical or radioactive tracers, capable of withstanding extreme well conditions and require no special handling. At the perforation or cluster level, these tracers provide more detailed measurements, adding a new dimension and host of applications not possible with previously existing measurements. Nanoparticle tracers offer crucial insight into geological information and variability. As the oil and gas industry seeks to improve efficiency and maximize recovery, these nanoparticles hold an enormous opportunity for an increasingly important role by delivering valuable insights into reservoir behavior. 

Given the cost, complexities and limitations of traditional methods, QuantumPro, Inc., envisioned using nanoparticle tracers, delivered through perforation charges, as an opportunity and innovation that the industry was ready for. The specific application—assessing perforation flow performance as discussed here—is one of the new approaches that is being assessed, successfully tested, and deployed as of writing. Nanoparticle tracer technology provides a new level of detail for evaluating well completion efficiency, exceeding the scale and detail of traditional measurements. 

UNIQUELY IDENTIFIABLE, INERT NANOPARTICLE TRACERS ENABLE WIDE APPLICATIONS 

QuantumPro’s FloTrac ultra-high-resolution nanoparticle tracers are configurable in up to 220 different, uniquely identifiable and inert variations, Fig. 1. This large portfolio of unique tracers enables broad applications that can extend to adjacent wells, to record cross-well communication—critical for optimizing well spacing—and to replace trial-and-error approaches with data-driven optimization.

Fig. 1. Size comparison of FloTrac tracers, compared to different sand particles.

 

Unlike liquid chemical tracers, every FloTrac nanoparticle tracer is compatible with both water and oil, requiring only a single tracer composition, regardless of the fluid stream, reducing costs considerably. Since the insoluble FloTrac tracers do not dissolve after deployment, operators can perform surface sampling for at least nine months—well beyond the capability of liquid chemical tracers. FloTrac tracers also maintain stability in temperatures up to 2,000 °F. 

The specially designed nanoparticles show broad application, and after laboratory testing, they were recently deployed via modified perforating charges by True Oil, LLC, in the Williston basin of North Dakota in a first-ever field trial with encouraging results. 

LABORATORY VALIDATION OF NANOPARTICLE TRACER APPLICATION TO PERFORATION SYSTEMS 

In 2023, researchers validated nanoparticle tracers and implementation methodology through comprehensive laboratory testing, in accordance with API RP19 standards, at the GEODynamics Inc. testing and manufacturing facility, located in Millsap, TX. Researchers added nanoparticle tracers to the perforation liner of the equal entry hole, FracIQ charge, Fig. 2

Fig. 2. Ultrahigh-resolution nanoparticles added to the perforation liner.

The test aimed to accomplish the following: 

  • Assess the stability of nanoparticle tracers under the extreme conditions typical of perforation charge detonation 
  • Determine if applying the nanoparticles had any impact on the perforation hole size and depth penetration, as well as how various nanoparticle concentrations impacted the respective measurements after charge detonation 
  • Confirm nanoparticle recovery, detectability and measured concentration 

The test confirmed that the nanoparticle tracers could withstand the extreme conditions of the perforation detonation. Importantly, the test concentrations of nanoparticles applied to the perforation liner had negligible impact on the expected depth of penetration and the entrance hole size—a crucial factor for maintaining charge performance. 

High-energy, sub-atomic X-ray analyses of fluid and solid particle samples, collected from the perforation tunnels inside the concrete cores, indicated high tracer recovery and favorable signaling characteristics across various charge types. The different tracer concentrations permitted selection of the optimal concentration to use in field deployments. Nanoparticle detection was confirmed and field testing enabled. 

After validating the approach with laboratory testing, researchers conducted a field trial to confirm real-world application of the nanoparticle tracers and delivery mechanism. 

FIELD TESTING VALIDATES APPLICATION AND METHODOLOGY 

Like the lab tests, the objective of the field trial was to explore various nanoparticle concentrations and verify measurable nanoparticle recovery, including surface recovery in the field trial. The field test also allowed for the application of nanoparticles to not just the perforation liner, but to other areas of the perforation system outlined. Phase 1 field testing was conducted in October 2024 in a True Oil, LLC-operated well in the Williston basin. 

The QuantumPro, Inc., team sent five unique nanoparticle tracers to the GEODynamics manufacturing facility for preparation and delivery to the wellsite. Prior preparation by the manufacturer eliminated the need for special work onsite, once the perforation guns arrived, other than placing the guns in pre-defined locations, since the nanoparticle tracers are uniquely identifiable and operators can link recovery to specific perforations or perforation clusters. The team designed a field test that identified well completion Stages 12 and 13 as representative stages for testing eight perforation clusters per stage. 

Fig. 3. An outline of the field test criteria identifying how the five unique tracers were deployed and the varying concentrations tested.

The field test included additional variability—beyond the lab test—to investigate a wider range of applications, including placing a relatively large volume of nanoparticle tracers in a vial within the gun, in the space available. As in the laboratory tests, varying nanoparticle tracer concentrations were applied to determine tracer recovery. Each stage consisted of eight clusters and each cluster was perforated with four shots. Tracer-embedded charges were deployed, using a standard plug-and-perf method, with manufacturing partner GEODynamics integrating the nanoparticle tracers during the manufacturing process, Fig. 3

 

RESULTS ENCOURAGE FOLLOW-UP TESTING 

Results demonstrated sufficient nanoparticle tracer recovery at the cluster level, facilitating advanced flow mapping, quantification of production, and flow performance verification for each individual cluster, Fig. 4

Fig. 4. The results and analysis of the flowback sample, taken one week after initial production.

Following the successful field trial, the team initiated a phase 2 field test, which is underway in a second True Oil well, where results will be available late in January 2025. As a further validation of the process and results, True Oil representative Wallace Hendricks commented that, “The ability to easily deploy and control the placement of individual tracers in specific zones along the lateral is a game changer.” He added, “In the field, deployment of the tracer was a seamless operation with wireline. No additional personnel or equipment was needed.” 

 

GROUNDBREAKING, COST-EFFECTIVE ADVANCEMENT IN PRODUCTION FLOW MONITORING 

The cluster-level flow monitoring technique signifies a groundbreaking advancement in the industry, providing cost-effective and nonintrusive means to assess perforation flow performance and inter-well communication. Furthermore, this technology allows operators to: 

  • Achieve cluster-level flow mapping resolution, providing further verification of perforation efficiency beyond step-down tests 
  • Verify perforation efficiency of multiple perf designs in a single well, to complement the results of, or reduce the reliance on additional diagnostics, such as cameras or fiberoptics 
  • Gain a better understanding of stage level contributions of geologic layers in areas that are out of zone 
  • Verify zonal isolation and plug and cement quality
  • Understand toe vs. middle heel contributions. 

The early deployment of nanoparticle tracers embedded in the perforation tunnel means that operators will have a better understanding, not only of which clusters are contributing, but also how the frac is distributed and contributing to the overall production of the well. 

The method’s applications extend to multi-stage completions in unconventional wells, offshore wells, enhanced geothermal system (EGS) wells and carbon capture, utilization and storage (CCUS) wells. The perforation level flow monitoring approach enhances clarity during the post-perforation analysis and reservoir development, offering critical insights for optimizing perforation design and overall completion strategies to maximize asset value and performance. 

ACKNOWLEDGMENT 

The authors sincerely thank Phil Snider and Steve Baumgartner, formerly of GEODynamics, whose support and contributions were instrumental to this technology. 

WALLACE HENDRICKS is a completion superintendent at True Oil LLC. He holds bachelor’s degrees in geophysics and civil engineering from the University of Wyoming. He is also a registered Professional Engineer in the State of Wyoming. 

 

 

 

ERIC MARSHALL is a petroleum engineer with 23 years of experience in the oil and gas industry, specializing in hydraulic fracturing and reservoir engineering. He currently serves as senior technical advisor at GEODynamics, where he identifies new technology and intellectual property to drive future growth. Prior to joining GEODynamics, Mr. Marshall held the position of vice president of Engineering at FractureID, where he established an engineering consultancy division. He also managed a global technical implementation team for a coiled tubing stimulation service at Halliburton across 11 countries. Mr. Marshall holds a bachelor’s degree in mechanical engineering from the Colorado School of Mines and is a registered Professional Petroleum Engineer in multiple states. He actively participates in professional organizations, such as SPE. 

 

TALGAT SHOKANOV is CEO of QuantumPro, Inc., which he founded in 2017, following a 15-year career at SLB. There, he held a variety of international and technology development assignments and previously spearheaded SLB’s cuttings re-injection via hydraulic fracturing business line, including subsurface engineering, disposal domain mapping and pressure diagnostics analysis. He holds numerous patents and has authored over 50 technical papers in complex fracturing and injection. He holds bachelor’s and master’s degrees in petroleum engineering from Satbayev University in Kazakhstan. 

 

JOHN OLIVER is a business advisor to QuantumPro Inc. He has over 45 years of experience in the oil and gas industry, including a number of senior executive positions with M-I SWACO, an SLB company. He managed all the segments in the South American business unit as senior VP and served as Global Marketing manager. Mr. Oliver went on to lead Prince Energy, a division of Prince International, from which he retired in July 2018. He currently serves on a number of boards and is an advisor to several companies and energy private equity investment firms. He holds a BS degree with honors in biochemistry from University of St. Andrews in Scotland.

 

QUAN GUO is a geomechanics advisor at QuantumPro, Inc. He was with M-I SWACO and later SLB from 2003 to 2022. Before M-I SWACO, he was with Advantek from 2000 to 2003 and TerraTek from 1992 to 2000. His experience includes perforating and hydraulic fracturing lab testing and modeling, drilling fluids and wellbore strengthening, cuttings and produced water re-injection. He holds 13 patents and has authored over 80 technical papers. He holds a bachelor’s degree in mathematics and mechanics from Lanzhou University, a master’s degree in engineering mechanics from Huazhong University of Science and Technology in China, and a Ph.D in mechanical engineering from Northwestern University in Evanston, IL. 

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